HCID 86678221, compound → HCID 71510292, compound

Participants

Reaction Steps

Intermediate 23 (68 mg, 0.09 mmol) was dissolved in 31% trimethylamine in ethanol (3 ml) and stirred at RT for 16 hours. The solvent was evaporated in vacuo, and the resulting residue repeatedly azeotroped with diethyl ether until a solid formed. The solid was collected and dried in vacuo to yield the title compound as an off-white solid (51 mg).

Provenance & Evidence