HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86673423, compound → HCID 86673427, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86673423 | HCID 86673423 | — |
| Reactant | HCID 86673425 | HCID 86673425 | — |
| Product | HCID 86673427 | HCID 86673427 | — |
Reaction Steps
Prepared according to the same procedure as diethyl 2,5-difluorobenzylphosphonate, starting with 4-(bromomethyl)-6-chloropyrimidine. 1H NMR (500 MHz, DMSO-d6) δ 9.00 (s, 1H), 7.68 (dd, J=2.3, 1.1 Hz, 1H), 4.21-3.88 (m, 4H), 3.74-3.45 (m, 2H), 1.20 (t, J=7.0 Hz, 6H), Mass spec.: 265.1 (MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691821B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-23693eeb618949c8a6bb5feeb8f65dbd |
| Source note | uspto-grants-2014_04 |