HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylethylamine → HCID 53252537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylethylamine | HCID 11723 | — |
| Reactant | HCID 67251903 | HCID 67251903 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 53252537 | HCID 53252537 | — |
Reaction Steps
Synthesis worked according to the preparation of A5-1 when using 340 mg (0.99 mmol) (S)-N-(8-methoxytetralin-2-yl)-N-propyl-2-(2-thienyl)acetamide ((S)-A4-1: R=OMe, Cy=2-thienyl). Flash chromatography was done using a mixture of hexane/ethyl acetate 40/1 in the presence of 0.5% (v/v) dimethylethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691839B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-6609108080a34f1c8a94c4c2f9d85022 |
| Source note | uspto-grants-2014_04 |