HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylethylamine → HCID 53253205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylethylamine | HCID 11723 | — |
| Reactant | HCID 53252573 | HCID 53252573 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 53253205 | HCID 53253205 | — |
Reaction Steps
Synthesis worked according to the preparation of A7-1 when using 21 mg (0.06 mmol) (R)-N-(8-methoxytetralin-2-yl)-N-propyl-N-[2-(2-thienyl)ethyl]amine ((R)-A5-1: R=OMe, Cy=2-thienyl). Flash chromatography was done using hexane/ethyl acetate 40/10 in the presence of 0.5% (v/v) dimethylethylamine to achieve compound 1a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691839B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-3d6fc9785c3b4d9991bb7b6ae5b2a4e9 |
| Source note | uspto-grants-2014_04 |