HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylethylamine → HCID 53252575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylethylamine | HCID 11723 | — |
| Reactant | HCID 53252537 | HCID 53252537 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 53252575 | HCID 53252575 | — |
Reaction Steps
Synthesis worked according to the preparation of A7-1 when using 76 mg (0.23 mmol) (S)-N-(8-methoxytetralin-2-yl)-N-propyl-N-[2-(2-thienyl)ethyl]amine ((S)-A5-1: R=OMe, Cy=2-thienyl). Flash chromatography was done using hexane/ethyl acetate 10/1 in the presence of 1% (v/v) of dimethylethylamine to achieve compound 1b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691839B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-984c7df09e8a408aa93cb713a1192b4a |
| Source note | uspto-grants-2014_04 |