Ethanol → HCID 136379487, compound

Participants

Reaction Steps

A suspension of Example 22A (0.118 g, 0.223 mmol), ethanol (3 mL), water (0.25 mL), hydroxylamine hydrochloride (0.039 g, 0.558 mmol), and triethylamine (0.140 mL, 1.0 mmol) was heated at 80° C. for 30 minutes. The reaction was cooled to ambient temperature, diluted with water (13 mL) and stirred 5 minutes. The suspension was filtered. The solid collected was washed with water and dried in a vacuum oven at 50° C. to provide the title compound. MS ESI(+) m/z 408.0 [M+H]+.

Provenance & Evidence