Fumaric Acid → HCID 20217031, compound

HRID 236278Notes

Reaction equation

HRID 236278 reaction equation
[N:1]1([C:6]2[S:10][C:9]([C:11]3[CH:12]([CH3:18])[CH2:13][C:14](=[O:17])[NH:15][N:16]=3)=[CH:8][CH:7]=2)[CH:5]=[CH:4][N:3]=[CH:2]1.[C:19]([OH:26])(=[O:25])/[CH:20]=[CH:21]/[C:22]([OH:24])=[O:23]>C(O)C>[C:19]([OH:26])(=[O:25])/[CH:20]=[CH:21]/[C:22]([OH:24])=[O:23].[N:1]1([C:6]2[S:10][C:9]([C:11]3[CH:12]([CH3:18])[CH2:13][C:14](=[O:17])[NH:15][N:16]=3)=[CH:8][CH:7]=2)[CH:5]=[CH:4][N:3]=[CH:2]1

Participants

4

Reactant 2

HCID 444972Fumaric AcidHCID 13318705HCID 13318705, compound

Product 1

HCID 20217031HCID 20217031, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 200 mg of 6-[5-(1-imidazolyl)-thien-2-yl]-5-methyl-3-oxo-2,3,4,5-tetrahydro-pyridazine and 89 mg of fumaric acid was heated in 50 ml ethanol until solution was effected. Then the solution was evaporated and the residue dried.

Workup

  1. customThen the solution was evaporated
  2. customthe residue dried

Sources & evidence

ORD record
ord-a84671f6992a42d4b7481caadfeef391
Source dataset
uspto-grants-1987_02
Patent number
US04643998

Reaction notes

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