3-(3-Nitrophenyl)prop-2-enal → 3-nitrocinnamaldehyde Thiosemicarbazone

HRID 2362834Notes

Reaction equation

HRID 2362834 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:11]=[CH:12][CH:13]=1)[CH:7]=[CH:8][CH:9]=O)([O-:3])=[O:2].[NH2:14][NH:15][C:16]([NH2:18])=[S:17]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:11]=[CH:12][CH:13]=1)[CH:7]=[CH:8][CH:9]=[N:14][NH:15][C:16]([NH2:18])=[S:17])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 2664543-(3-Nitrophenyl)prop-2-enalHCID 2723789Thiosemicarbazide

Product 1

HCID 866333063-nitrocinnamaldehyde ThiosemicarbazoneYield 88%

Procedure

The compound is prepared according to the method described in Example 1A from 3-nitrocinnamaldehyde (2.2 mmol) (Org. Lett. 5(5), 777-780, 2003) and from thiosemicarbazide (2.2 mmol). Yield 88%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-40a79d62a0e649a2bb29c23a3e779dba
Source dataset
uspto-grants-2014_04
Patent number
US08691854B2

Reaction notes

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