2-Propenal, 3-(2-methoxyphenyl)- → HCID 57221575, compound

HRID 2362835Notes

Reaction equation

HRID 2362835 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][CH:10]=[CH:9][C:4]=1[CH:5]=[CH:6][CH:7]=O.[NH2:13][NH:14][C:15]([NH2:17])=[S:16]>>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][CH:10]=[CH:9][C:4]=1[CH:5]=[CH:6][CH:7]=[N:13][NH:14][C:15]([NH2:17])=[S:16]

Participants

3

Reactant 2

HCID 151732-Propenal, 3-(2-methoxyphenyl)-HCID 2723789Thiosemicarbazide

Product 1

HCID 57221575HCID 57221575, compoundYield 45%

Procedure

The compound is prepared according to the method described in Example 1A from 2-methoxycinnamaldehyde (6 mmol) and from thiosemicarbazide (6 mmol). Yield 45%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-960fc6919f43488f9ffc8b834016349f
Source dataset
uspto-grants-2014_04
Patent number
US08691854B2

Reaction notes

Loading…