HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4'-(trifluoromethyl)acetophenone → HCID 86633307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4'-(trifluoromethyl)acetophenone | HCID 321979 | — |
| Reactant | Cinnamaldehyde, thiosemicarbazone | HCID 2737765 | — |
| Product | HCID 86633307 | HCID 86633307 | 42% |
Reaction Steps
The compound is prepared according to the method described in Example 1B from cinnamaldehyde thiosemicarbazone (0.5 mmol) (Eur. J. Med. Chem. 25(7), 581-588, 1990) and from 2-bromo-4′-trifluoromethylacetophenone (0.5 mmol) (Tet., 59(8) 1317-1325, 2003). Yield 42%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691854B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-1230b79c1ad641c8ad14a8d518784cb5 |
| Source note | uspto-grants-2014_04 |