2-Propenal, 3-(3-methoxyphenyl)-, (2E)- → HCID 86633308, compound

HRID 2362837Notes

Reaction equation

HRID 2362837 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][CH:12]=1)[CH:6]=[CH:7][CH:8]=O.[NH2:13][NH:14][C:15]([NH2:17])=[S:16]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][CH:12]=1)[CH:6]=[CH:7][CH:8]=[N:13][NH:14][C:15]([NH2:17])=[S:16]

Participants

3

Reactant 2

HCID 5956962-Propenal, 3-(3-methoxyphenyl)-, (2E)-HCID 2723789Thiosemicarbazide

Product 1

HCID 86633308HCID 86633308, compoundYield 52%

Procedure

The compound is prepared according to the method described in Example 1A from 3-methoxycinnamaldehyde (2.47 mmol) and from thiosemicarbazide (2.47 mmol). Yield 52%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-73e5a4c84cc4483684a3b8f710a3bfea
Source dataset
uspto-grants-2014_04
Patent number
US08691854B2

Reaction notes

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