Thiosemicarbazide → HCID 86633309, compound

HRID 2362838Notes

Reaction equation

HRID 2362838 reaction equation
[CH3:1][C:2]1[CH:11]=[CH:10][CH:9]=[CH:8][C:3]=1[CH:4]=[CH:5][CH:6]=O.[NH2:12][NH:13][C:14]([NH2:16])=[S:15]>>[CH3:1][C:2]1[CH:11]=[CH:10][CH:9]=[CH:8][C:3]=1[CH:4]=[CH:5][CH:6]=[N:12][NH:13][C:14]([NH2:16])=[S:15]

Participants

3

Reactant 2

HCID 2723789ThiosemicarbazideHCID 534274143-(2-Methylphenyl)-2-propenal

Product 1

HCID 86633309HCID 86633309, compoundYield 42%

Procedure

The compound is prepared according to the method described in Example 1A from 2-methylcinnamaldehyde (0.27 mmol) and from thiosemicarbazide (0.27 mmol). Yield 42%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-5f510b972f22485ea5abb2c74784f10e
Source dataset
uspto-grants-2014_04
Patent number
US08691854B2

Reaction notes

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