Thiosemicarbazide → HCID 86633310, compound

HRID 2362839Notes

Reaction equation

[C:1]([C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][CH:12]=1)[CH:6]=[CH:7][CH:8]=O)#[N:2].[NH2:13][NH:14][C:15]([NH2:17])=[S:16]>>[C:1]([C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][CH:12]=1)[CH:6]=[CH:7][CH:8]=[N:13][NH:14][C:15]([NH2:17])=[S:16])#[N:2]

Participants

Reactant 2

HCID 2723789Thiosemicarbazide

HCID 544772143-Cyano-1-(2-formylethenyl)benzene

Product 1

HCID 86633310HCID 86633310, compoundYield 46%

Procedure

The compound is prepared according to the method described in Example 1A from 3-cyanocinnamaldehyde (2.54 mmol) and from thiosemicarbazide (2.54 mmol). Yield 46%.

Workup

customThe compound is prepared

Sources & evidence

ORD record: ord-d03973d8ab61481d9648bfd659859d7b
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08691854B2

Reaction notes

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