Thiosemicarbazide → HCID 86633311, compound

HRID 2362840Notes

Reaction equation

[Cl:1][C:2]1[CH:11]=[CH:10][CH:9]=[CH:8][C:3]=1[CH:4]=[CH:5][CH:6]=O.[NH2:12][NH:13][C:14]([NH2:16])=[S:15]>>[Cl:1][C:2]1[CH:11]=[CH:10][CH:9]=[CH:8][C:3]=1[CH:4]=[CH:5][CH:6]=[N:12][NH:13][C:14]([NH2:16])=[S:15]

Participants

Reactant 2

HCID 2723789Thiosemicarbazide

HCID 30140422-Chlorocinnamaldehyde

Product 1

HCID 86633311HCID 86633311, compoundYield 55%

Procedure

The compound is prepared according to the method described in Example 1A from 2-chlorocinnamaldehyde (0.15 mmol) and from thiosemicarbazide (0.15 mmol). Yield 55%.

Workup

customThe compound is prepared

Sources & evidence

ORD record: ord-f5912bd7deb74c2ebe1cbe618271d162
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08691854B2

Reaction notes

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