Thiosemicarbazide → HCID 86633315, compound

HRID 2362844Notes

Reaction equation

HRID 2362844 reaction equation
[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([CH:12]=[CH:13][CH:14]=1)[CH:8]=[CH:9][CH:10]=O)(=[O:4])=[O:3].[NH2:15][NH:16][C:17]([NH2:19])=[S:18]>>[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([CH:12]=[CH:13][CH:14]=1)[CH:8]=[CH:9][CH:10]=[N:15][NH:16][C:17]([NH2:19])=[S:18])(=[O:4])=[O:3]

Participants

3

Reactant 2

HCID 2723789ThiosemicarbazideHCID 86633316HCID 86633316, compound

Product 1

HCID 86633315HCID 86633315, compoundYield 70%

Procedure

The compound is prepared according to the method described in example 1A from 3-methylsulfonylcinnamaldehyde (3.8 mmoles) and from thiosemicarbazide (3.8 mmoles). Yield 70%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-0ae3f54a65d94ade8ad0ea9617387e4b
Source dataset
uspto-grants-2014_04
Patent number
US08691854B2

Reaction notes

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