Thiosemicarbazide → HCID 86633320, compound

HRID 2362847Notes

Reaction equation

HRID 2362847 reaction equation
[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][CH:12]=1)[CH:6]=[CH:7][CH:8]=O.[NH2:13][NH:14][C:15]([NH2:17])=[S:16]>>[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][CH:12]=1)[CH:6]=[CH:7][CH:8]=[N:13][NH:14][C:15]([NH2:17])=[S:16]

Participants

3

Reactant 2

HCID 2723789ThiosemicarbazideHCID 91440219HCID 91440219, compound

Product 1

HCID 86633320HCID 86633320, compoundYield 25%

Procedure

The compound is prepared according to the method described in example 1A from 3-hydroxymethylcinnamaldehyde (3 mmoles) et de thiosemicarbazide (3 mmoles). Yield 25%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-39ba9f23937c41a199fe9b8c55442bb6
Source dataset
uspto-grants-2014_04
Patent number
US08691854B2

Reaction notes

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