Thiosemicarbazide → HCID 91516711, compound

HRID 2362849Notes

Reaction equation

HRID 2362849 reaction equation
[F:1][C:2]1[CH:11]=[CH:10][C:5]([CH:6]=[CH:7][CH:8]=O)=[CH:4][CH:3]=1.[NH2:12][NH:13][C:14]([NH2:16])=[S:15]>>[F:1][C:2]1[CH:11]=[CH:10][C:5]([CH:6]=[CH:7][CH:8]=[N:12][NH:13][C:14]([NH2:16])=[S:15])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 2723789ThiosemicarbazideHCID 533843793-(4-Fluorophenyl)-2-propenal

Product 1

HCID 91516711HCID 91516711, compoundYield 53%

Procedure

The compound is prepared according to the method described in example 1A from 4-fluorocinnamaldehyde (1.5 mmoles) and from thiosemicarbazide (1.5 mmoles). Yield 53%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-802e33c4d5ef4fce98fe3ab51c18a044
Source dataset
uspto-grants-2014_04
Patent number
US08691854B2

Reaction notes

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