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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2363145Generated: October 30, 2026

HCID 58319312, compound → HCID 58319227, compound

https://huagongshe.com/reaction/2363145

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58319312HCID 58319312—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
SolventEthyl AcetateHCID 8857—
ProductHCID 58319227HCID 5831922789%

Reaction Steps

A mixture of 1-(3-methoxy-phenyl)-cyclobutanol and 10% Pd/C (60 mg) in ethanol (10 ml) was hydrogenated under 45 psi hydrogen atmosphere for 3 hours. The mixture was diluted with EtOAc, filtered through a celite pad. The filtrate was concentrated under reduced pressure, and dried to give 1-cyclobutyl-3-methoxy-benzene (162 mg, 89%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08691855B2
Source datasetuspto-grants-2014_04
ORD IDord-f29b250a7504402a80cd3b225669cda4
Source noteuspto-grants-2014_04