HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → n-(2,3-Dihydro-benzo[1,4]dioxin-2-ylmethyl)-formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | 2-Aminomethyl-1,4-benzodioxane | HCID 15053 | — |
| Product | n-(2,3-Dihydro-benzo[1,4]dioxin-2-ylmethyl)-formamide | HCID 64990658 | — |
Reaction Steps
Racemic 2,3-dihydro-1,4-benzdioxin-2-ylmethylamine (825 mg, 5 mmol) was dissolved in ethyl formate (15 mL), refluxed for 30 min and evaporated in vacuo to yield N-(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-formamide as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691867B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-741843c2a1ff44079465a6e2f6f79cb3 |
| Source note | uspto-grants-2014_04 |