(Z)-1-Ethoxy-2-(tributylstannyl)ethene → HCID 68778467, compound

HRID 2363715Notes

Reaction equation

HRID 2363715 reaction equation
Br[CH2:2][C:3]([C:5]1[CH:6]=[CH:7][C:8]2[N:9]([CH:11]=[C:12]([C:14]([NH:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[O:15])[N:13]=2)[CH:10]=1)=O.C([Sn](CCCC)(CCCC)[CH:28]=[CH:29][O:30]CC)CCC>>[CH2:29]([O:30][CH:2]=[CH:3][C:5]1[CH:6]=[CH:7][C:8]2[N:9]([CH:11]=[C:12]([C:14]([NH:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[O:15])[N:13]=2)[CH:10]=1)[CH3:28]

Participants

3

Reactant 2

HCID 2763294(Z)-1-Ethoxy-2-(tributylstannyl)etheneHCID 44136066HCID 44136066, compound

Product 1

HCID 68778467HCID 68778467, compound

Procedure

This product is obtained under conditions similar to those described in the first step of preparation of Intermediate 9, replacing the tributyl(1-ethoxyvinyl)tin with tributyl(2-ethoxyvinyl)tin.

Workup

  1. customThis product is obtained under conditions similar to

Sources & evidence

ORD record
ord-f2e252552f0e4a5792adff7f2bf33374
Source dataset
uspto-grants-2014_04
Patent number
US08691990B2

Reaction notes

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