HRID236383

反应详情

EQUATION

反应方程式

HRID 236383 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A 0.3% solution of 0.2 g of poly(isobutylene-co-isoprene) was prepared in 99.7% of a 1:2 mixture of 2,2,4-trimethylpentane and CCl4. The solution was purged with N2, heated to 75 C., 0.09 g of azobisisobutyronitrile was added, followed by 5 g of methylmethacrylate, added over a period of one half hour. The polymerization was carried out for 8 hours with constant mechanical stirring, under a N2 atmosphere. After cooling the reaction mixture to room temperature, the cleaning procedure used was identical to that of Example 1.

WORKUP

后处理

  1. customThe solution was purged with N2
  2. temperatureheated to 75 C
  3. addition, 0.09 g of azobisisobutyronitrile was added
  4. additionadded over a period of one half hour