Methyl Anthranilate → HCID 178497644, compound

Participants

Reaction Steps

A mixture was prepared from 12.2 g of 5-aminotetrazole monohydrate, 71.3 g of triethoxymethane, 22.3 g of methyl anthranilate and 100 ml of carbon tetrachloride and this was refluxed under nitrogen with stirring for 16 hours. The mixture was then cooled to room temperature and the white crystals which formed were separated by filtration, washed with carbon tetrachloride and dried to give N1 -(1H-tetrazol-5-yl)-N2 -(2-carbomethoxyphenyl)formamidine melting at about 199°-200° C.

Provenance & Evidence