2-Methoxyethylamine → HCID 54685340, compound

Participants

Reaction Steps

This compound was prepared from ethyl 4-hydroxy-1-[(4-nitrophenyl)methyl]-2-oxo-7-(phenylmethyl)-1,2-dihydro-1,5-naphthyridine-3-carboxylate and 2-methoxyethylamine employing methods similar to those described in Example 2 and was obtained as a light yellow solid: 1H NMR (d6-DMSO) δ 10.69 (1H, br), 8.21 (1H, s), 8.10 (2H, d, J=8.7 Hz), 7.35 (2H, d, J=8.7 Hz), 7.31 (1H, s), 7.13 (3H, m), 7.07 (2H, m), 5.49 (2H, br s), 3.91 (2H, s), 3.41 (4H, m), 3.27 (3H, s); HRMS calcd for C26H24N4O6+H+: 489.1774. Found: 489.1778.

Provenance & Evidence