2-Phenoxyethanamine → HCID 86762319, compound

Participants

Reaction Steps

This compound was prepared from ethyl 7-[(4-fluorophenyl)methyl]-4-hydroxy-2-oxo-1,2-dihydro-1,5-naphthyridine-3-carboxylate and 2-phenoxyethylamine employing methods similar to those described in Example 2 and was obtained as a white solid: 1H NMR (d6-DMSO) δ 11.85 (1H, br s), 10.49 (1H, br s), 8.49 (1H, br s), 7.42 (1H, br s), 7.32-7.25 (4H, m), 7.14 (2H, t, J=8.7 Hz), 6.97-6.91 (3H, m), 4.14-4.08 (4H, br m), 3.72 (2H, br); HRMS calcd for C24H20FN3O4+H+: 434.1516. Found 434.1519.

Provenance & Evidence