Ethoxyethylamine → HCID 69481523, compound

Participants

Reaction Steps

This compound was prepared from ethyl 7-[(4-fluorophenyl)methyl]-4-hydroxy-2-oxo-1,2-dihydro-1,5-naphthyridine-3-carboxylate and 2-ethoxyethylamine employing methods similar to those described in Example 2 and was obtained as a white solid: 1H NMR (d6-DMSO) δ 11.82 (1H, br s), 10.58 (1H, br s), 8.19 (1H, br s), 7.35-7.26 (3H, m), 7.15-7.10 (2H, m), 4.03 (2H, br s), 3.48-3.41 (6H, m), 1.11 (3H, t, J=8.4 Hz); HRMS calcd for C20H20FN3O4+H+: 386.1516. Found 386.1501.

Provenance & Evidence