HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilanol → Hexamethyldisiloxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilanol | HCID 66110 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Hexamethyldisiloxane | HCID 24764 | — |
Reaction Steps
This reaction proceeds slowly without diethylether but reacts faster at reflux temperatures. Trimethylsilanol is condensed during the HMDS distillation step to give HMDSO, which reacts as shown above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04644076 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-5481fd3911d649d58cd82ef099a34174 |
| Source note | uspto-grants-1987_02 |