2-(Propan-2-yloxy)ethan-1-amine → HCID 69482818, compound

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Reaction Steps

This compound was prepared from ethyl 7-[(4-fluorophenyl)methyl]-4-hydroxy-2-oxo-1,2-dihydro-1,5-naphthyridine-3-carboxylate and 2-aminoethylisopropylether employing methods similar to those described in Example 2 and was obtained as a white solid: 1H NMR (d6-DMSO) δ 11.72 (1H, br s), 10.88 (1H, br s), 10.06 (1H, br s), 8.18 (1H, s), 7.30-7.25 (3H, m), 7.16-7.11 (2H, m), 3.98 (2H, br s), 3.57-3.54 (1H, m), 3.50-3.38 (4H, m), 1.08 (6H, d, J=5.7 Hz); HRMS calcd for C21H22FN3O4+H+: 400.1667. Found 400.1673.

Provenance & Evidence