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HRID236443

反应详情

EQUATION

反应方程式

HRID 236443 的结构方程式

REACTANTS

反应物

4
结构：II
HCID807

Iodine

I2

结构：ClCc1cccc(Cl)c1
HCID12103

alpha,3-Dichlorotoluene

C7H6Cl2

结构：CC(=O)[O-].[Na+]
HCID517045

Sodium Acetate

C2H3NaO2

结构：CNc1cccc(F)c1
HCID2759011

3-Fluoro-N-methylaniline

C7H8FN

PRODUCTS

生成物

1
结构：CN(Cc1cccc(Cl)c1)c1cccc(F)c1
HCID14008650

未命名化合物

PROCEDURE

实验过程

N-methyl-N-m-chlorobenzyl-m-fluoroaniline was prepared from 17.5 grams (0.14 mole) of N-methyl-m-fluoroaniline, 23. grams (0.14 mole) m-chlorobenzyl chloride (Aldrich), 11.9 grams anhydrous sodium acetate and 0.12 grams iodine according to the procedure described in Example III. Yield 28.6 grams (83.7 percent), boiling point 172° C. at 0.07 mmHg.