huagongshe.com
HRID236473

反应详情

EQUATION

反应方程式

HRID 236473 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)O
HCID6386

tert-Butyl alcohol

C4H10O

结构：CCCCCCCCCCCCCCCC(O)=C1C(=O)OC(C)(C)OC1=O
HCID54697955

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCCC(=O)CC(=O)OC(C)(C)C
HCID16110963

未命名化合物

收率 99.8%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

2,2-Dimethyl-5-(1-hydroxyhexadecylidene)-1,3-dioxane-4,6-dione (200 g) and tert-butyl alcohol (170 g) were refluxed in benzene (1 l) for 4 hours. Evaporation of the solvent gave crude tert-butyl 3-oxooctadecanoate (185 g) as an oil.

WORKUP

后处理

  1. customEvaporation of the solvent