HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethyl-1,3-dioxane-4,6-dione → 5-(1-Hydroxy-9-octadecenylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| Reactant | 9-Octadecenoyl chloride | HCID 66987 | — |
| Product | 5-(1-Hydroxy-9-octadecenylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 70446691 | 88.4% |
Reaction Steps
Starting from 9-octadecenoyl chloride (15 g) and 2,2-dimethyl-1,3-dioxane-4,6-dione (8 g), 5-(1-hydroxy-9-octadecenylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione (18 g) was obtained as an oil according to similar manner to that of Preparation A-2 (1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04643990 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-68e0134ec28c4b85b1e33175bd8aa9d9 |
| Source note | uspto-grants-1987_02 |