HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178479713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178451943 | HCID 178451943 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178479713 | HCID 178479713 | — |
Reaction Steps
Dissolved the product from Example 39H (350 mg, 0.458 mmol) in 4M hydrochloric acid in dioxane solution (6 mL) and stirred the solution at room temperature for 30 min then concentrated the mixture under high vacuum to a solid (approx. 310 mg) as a hydrochloride salt that was used directly in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691938B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-9f595549bce5423384b67eaba54bb5f1 |
| Source note | uspto-grants-2014_04 |