HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Glutamic acid dibenzyl ester → dibenzyl N-[N-(3-hexadecanoyloxyoctadecanoyl)-5-aminopentanoyl]-L-glutamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Glutamic acid dibenzyl ester | HCID 3037947 | — |
| Reactant | 5-(3-Hexadecanoyloxyoctadecanoyl)aminovaleric acid | HCID 13371863 | — |
| Product | dibenzyl N-[N-(3-hexadecanoyloxyoctadecanoyl)-5-aminopentanoyl]-L-glutamate | HCID 18606669 | 79.7% |
Reaction Steps
Starting from N-(3-hexadecanoyloxyoctadecanoyl)-5-aminopentanoic acid (1.27 g) prepared by the method of Preparation B-6 and dibenzyl L-glutamate (0.65 g), dibenzyl N-[N-(3-hexadecanoyloxyoctadecanoyl)-5-aminopentanoyl]-L-glutamate (1.5 g) was obtained as crystal according to a similar manner to that of Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04643990 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-09808bbfc13041a89eaba08b4e5c20ec |
| Source note | uspto-grants-1987_02 |