HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-oxindole → HCID 86637671, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-oxindole | HCID 611193 | — |
| Reactant | 5-(2-diethylaminoethyl)-3-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridine-2-carbaldehyde | HCID 25023015 | — |
| Product | HCID 66607579 | HCID 66607579 | — |
| Product | HCID 86637671 | HCID 86637671 | 98.7% |
Reaction Steps
The title compound was prepared under the same conditions as described in Example 1 with 5-(2-diethylamino-ethyl)-3-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridine-2-carbaldehyde and 5-bromo-1,3-dihydro-indole-2-one (commercially available from Aldrich) as starting materials to give 2-(5-bromo-2-oxo-1,2-dihydro-indol-3-ylidenemethyl)-5-2-diethylamino-ethyl)-3-methyl-1,5,6,7-tetrahydro-pyrrolo[3,2-c]pyridin-4-one (56 mg, 98.7%) as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697692B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-85cf8435036d48ff9dd1b8e27b0441c8 |
| Source note | uspto-grants-2014_04 |