HuagongsheHuagongshe Chemistry Print Report · For research reference only
epsilon-(Benzyloxycarbonyl)-L-lysine → HCID 86741315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | epsilon-(Benzyloxycarbonyl)-L-lysine | HCID 1715626 | — |
| Reactant | Nalpha-(3-hexadecanoyloxyoctadecanoyl)-Nepsilon-benzyloxycarbonyl-L-lysine | HCID 70533277 | — |
| Product | HCID 86741315 | HCID 86741315 | 67.8% |
Reaction Steps
Starting from N-hydroxysuccinimide ester of Nα -(3-hexadecanoyloxyoctadecanoyl)-Nε -benzyloxycarbonyl-L-lysine (3 g) prepared by the method described in Example 20 (1), and Nε -benzyloxycarbonyl-L-lysine (2.24 g), Nα -[Nα -(3-hexadecanoyloxyoctadecanoyl)-Nε -benzyloxycarbonyl-L-lysyl]-Nε -benzyloxycarbonyl-L-lysine (2.7 g) was obtained as crystals according to a similar manner to that of Example 16 (2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04643990 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-b087f1b601174045bf9e00628e47669c |
| Source note | uspto-grants-1987_02 |