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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2365282Generated: November 1, 2026

HCID 59625758, compound → HCID 59625748, compound

https://huagongshe.com/reaction/2365282

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59625758HCID 59625758—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
ProductHCID 59625748HCID 59625748160.9%

Reaction Steps

A mixture of compound 8e (1.7 g, 2.9 mmol), and 10% Palladium on carbon (300 mg) was hydrogenated (50 psi hydrogen gas) using a Parr apparatus for 18 h. The catalyst was removed by filtration, and the solvent concentrated under reduced pressure to afford crude compound 8f (1.5 g). MS m/z (M+H+) 322.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08697684B2
Source datasetuspto-grants-2014_04
ORD IDord-61d5d0ae900d4fb5a67af4ff2c41ff73
Source noteuspto-grants-2014_04