HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 49782271, compound → HCID 49781583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 49782271 | HCID 49782271 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 49781583 | HCID 49781583 | 99.1% |
Reaction Steps
To a solution of compound 348 (30 mg) in EtOH (20 mL) was added 10% Pd/C (10 mg) and the mixture was subjected to hydrogenation (45 psi H2) for 1.5 h. The reaction mixture was filtered and the filtrate was concentrated under reduced pressure to give compound 349 (30 mg). MS m/z (M+H+) 460.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697684B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-60640dde805846c185e749eed86a605b |
| Source note | uspto-grants-2014_04 |