HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 49763995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 59625903 | HCID 59625903 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 49763995 | HCID 49763995 | 139% |
Reaction Steps
To a suspension of compound 17a (100 mg) and K2CO3 (69 mg) in MeCN was added compound 18a (0.0353 mL) and the mixture was stirred at room temperature for 30 min. The reaction was concentrated and the residue was diluted with EtOAc and water. The organics were concentrated and purified by flash column chromatography (silica gel, 8% MeOH/EtOAc) to afford compound 355 (85 mg). MS m/z (M+H+) 495.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697684B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-41649c268663450399774b0694daf7d4 |
| Source note | uspto-grants-2014_04 |