HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiomorpholine → HCID 59625692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiomorpholine | HCID 67164 | — |
| Reactant | Methyl 4-chloroquinazoline-7-carboxylate | HCID 17750389 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59625692 | HCID 59625692 | 10.3% |
Reaction Steps
A solution of methyl 4-chloroquinazoline-7-carboxylate 66a (1.01 mmol, 225 mg) and thiomorpholine 66b (2.02 mmol, 208 mg) in MeOH (1.6 mL) was refluxed overnight. Compound 66c (30 mg) was isolated after purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697684B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-86bb7410da6b43f8b486101627034cda |
| Source note | uspto-grants-2014_04 |