Triethylamine → HCID 20044184, compound

Participants

Reaction Steps

To a solution of the resultant compound of Example 76 (1.0 mmol) and triethyl amine (2.0 mmol) in chloroform (10 ml) cooled to 0° C. was added isovaleryl chloride (1.0 mmol) in CHCl3 (2 ml). After 3 h, the solution was washed sequentially with 10% citric acid, saturated NaHCO3, and brine. Drying and evaporating provided the desired compound.

Provenance & Evidence