HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67423178, compound → HCID 46214027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67423178 | HCID 67423178 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 46214027 | HCID 46214027 | — |
Reaction Steps
In a 10 ml round-bottomed flask, 0.2 g of 3-(2,4-bis(benzyloxy)phenyl)azetidine-1-carboxylic acid pentylamide is dissolved in 6 ml of methanol in the presence of 0.1 g of palladium-on-charcoal at 10%. The reaction mixture is stirred for 6 hours under a hydrogen atmosphere. The reaction mixture is filtered and the residue is then chromatographed on silica gel (95/5 dichloromethane/methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697726B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-9716ad53ca1948719712f1433c0cbde1 |
| Source note | uspto-grants-2014_04 |