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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2365902Generated: October 31, 2026

HCID 67423178, compound → HCID 46214027, compound

https://huagongshe.com/reaction/2365902

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67423178HCID 67423178—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 46214027HCID 46214027—

Reaction Steps

In a 10 ml round-bottomed flask, 0.2 g of 3-(2,4-bis(benzyloxy)phenyl)azetidine-1-carboxylic acid pentylamide is dissolved in 6 ml of methanol in the presence of 0.1 g of palladium-on-charcoal at 10%. The reaction mixture is stirred for 6 hours under a hydrogen atmosphere. The reaction mixture is filtered and the residue is then chromatographed on silica gel (95/5 dichloromethane/methanol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08697726B2
Source datasetuspto-grants-2014_04
ORD IDord-9716ad53ca1948719712f1433c0cbde1
Source noteuspto-grants-2014_04