HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → Hydrogen Bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-(2-Methoxyphenyl)piperidine | HCID 12937930 | — |
| Product | Hydrogen Bromide | HCID 260 | — |
| Product | 2-(Piperidin-3-yl)phenol | HCID 20502633 | — |
Reaction Steps
HBr was prepared by heating 3-(2-methoxyphenyl)piperidine.HCl (46 mg, 0.20 mmol) with 48% HBr in a microwave reactor at 120° C. for one hour. After evaporation, 61 mg of the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697723B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-a7d90583842441e9a4cad54e9603f879 |
| Source note | uspto-grants-2014_04 |