HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66726956, compound → 1106938-11-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66726956 | HCID 66726956 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1106938-11-7 | HCID 25175001 | 47.8% |
Reaction Steps
(R)-2,3-Dihydrobenzo[1,4]dioxin-2-yl-[(R*)-3-(3-hydroxyphenyl)piperidin-1-yl]-methanone (17.8 g, 54.7 mmol) was treated with BH3 THF according to the above general procedure. Crystallisation from hot EtOH gave 8.5 g of the title compound as almost white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697723B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-f9c8dbd5788645d3ace9be16b2cb56e9 |
| Source note | uspto-grants-2014_04 |