HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → N-tert-butyl-6-hydrazino-N-methylpyridine-3-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | N-tert-butyl-6-chloro-N-methylpyridine-3-sulfonamide | HCID 86659955 | — |
| Product | N-tert-butyl-6-hydrazino-N-methylpyridine-3-sulfonamide | HCID 67456669 | 84% |
Reaction Steps
According to the process described in Example 4.2, starting with 0.66 g (2.53 mmol) of N-tert-butyl-6-chloro-N-methylpyridine-3-sulfonamide and 0.46 mL of hydrazine monohydrate, 0.55 g of N-tert-butyl-6-hydrazino-N-methylpyridine-3-sulfonamide is obtained in the form of a white solid, which is used without further purification in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697731B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-760e306829b447c4a0a47a902c5e1af1 |
| Source note | uspto-grants-2014_04 |