HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic acid, [3-(bromoacetyl)phenyl]-, ethyl ester → HCID 178419570, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic acid, [3-(bromoacetyl)phenyl]-, ethyl ester | HCID 20216369 | — |
| Reactant | HCID 178513045 | HCID 178513045 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178419570 | HCID 178419570 | 94.9% |
Reaction Steps
A mixture of 17.17 gm of ethyl N-[3-(2-bromoacetyl)-phenyl]-carbamate, 7.1 gm of amidinothiourea and 45 ml of ethanol was refluxed for 4 hours and then cooled to room temperature. The precipitate formed thereby was filtered off and washed with cold ethanol, yielding 22 gm of the title compound, m.p. 240°-2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04645841 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-6d885af43e5a42df8c8026180f6c9d4f |
| Source note | uspto-grants-1987_02 |