HRID236643

反应详情

EQUATION

反应方程式

HRID 236643 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 9.33 gm of 2-guanidino-4-(3-amino-phenyl)-thiazole and 3.93 gm of ethyl N-cyano-formamidate in 65 ml of ethanol was stirred at room temperature overnight. The crystalline product which separated out was collected by filtration, washed with cold ethanol and dried, yielding 9.2 gm of the title compound, m.p. 215° C. (dec.)

WORKUP

后处理

  1. customThe crystalline product which separated out
  2. filtrationwas collected by filtration
  3. washwashed with cold ethanol
  4. customdried