HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridin-2-ylbenzaldehyde → HCID 16665466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridin-2-ylbenzaldehyde | HCID 1515240 | — |
| Reactant | 2,3-Diaminobenzamide dihydrochloride | HCID 53422807 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16665466 | HCID 16665466 | — |
Reaction Steps
A mixture of 2,3-diaminobenzamide dihydrochloride (1 g), 4-pyridin-2-ylbenzaldehyde (0.82 g) and 10% Pd/C (0.3 g) in methanol (30 mL) at reflux was stirred for 18 hours, cooled, filtered through diatomaceous earth (Celite®) and concentrated. The concentrate was crystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697736B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-8461bdab4ad64985bf8947bbc18ed842 |
| Source note | uspto-grants-2014_04 |