HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 70411455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 131715066 | HCID 131715066 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70411455 | HCID 70411455 | 31% |
Reaction Steps
4 g of the ester prepared in this manner were dissolved in 140 ml of methanol, and the solution was refluxed with 16.4 ml of 1M KOH for 1.5 hours. Working up by a procedure similar to that described in Example 1c gave the desired (S)-chromanyl ethanol in a yield of 31% of theory, based on racemic chromanol used.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04645845 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-41411f02ba834024af0bf0087f0eb331 |
| Source note | uspto-grants-1987_02 |