Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 57447018 | HCID 57447018 | — |
| Product | HCID 69506822 | HCID 69506822 | — |
Reaction Steps
The method described in Part D of Example 3 was used to treat ethyl 6-(2-propyl-1H-imidazo[4,5-c]quinolin-1-yl)hexanoate (5.0 g, 14 mmol) with methylamine (8 mL of a 40% solution). The reaction was complete after being stirred overnight at 70° C. Following the work-up procedure, 3.42 g of N-methyl-6-(2-propyl-1H-imidazo[4,5-c]quinolin-1-yl)hexanamide were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08697873B2 |
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| Source dataset | uspto-grants-2014_04 |
|---|
| ORD ID | ord-cb746ba03ece426e93d816eb51ad0927 |
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| Source note | uspto-grants-2014_04 |
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