反应详情

This compound was prepared from 700 mg. (1.99 mmol) of the end product of Example 9 and dimethylamine according to a procedure similar to that described above in Example 11. The reaction mixture was heated to 60°-65° in a sealed glass bomb for 16 hours. Recrystallization from acetone/ether/hexane yielded the desired end product: mp 176°-178°.

1. customThis compound was prepared from 700 mg
2. temperatureThe reaction mixture was heated to 60°-65° in a sealed glass bomb for 16 hours
3. customRecrystallization from acetone/ether/hexane
4. customyielded the desired end product