HCID 86736566, compound → HCID 21315885, compound

HRID 236793Notes

Reaction equation

HRID 236793 reaction equation
[C:1]1([S:7][CH:8]([C:12]2[CH:17]=[CH:16][C:15]([Cl:18])=[CH:14][CH:13]=2)[C:9]([NH2:11])=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>CO>[Cl:18][C:15]1[CH:16]=[CH:17][C:12]([C:8]2[S:7][C:1]3[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=3[C:9]=2[N:11]([CH2:9][CH2:8][CH2:12][CH3:13])[CH2:6][CH2:1][CH2:2][CH3:3])=[CH:13][CH:14]=1

Participants

3

Reactant 1

HCID 86736566HCID 86736566, compound

Product 1

HCID 21315885HCID 21315885, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Proceed as in Example 31 starting from the N,N-di(n-butyl) [α-phenylthioα-(4-chlorophenyl] acetamide (yellow oil boiling between 180° and 185° at 0.05 torr). The duration of reaction is 9 hours. 50% of theory of colourless prisms melting between 48° and 50° (methanol) are obtained.

Workup

  1. customThe duration of reaction
  2. custommelting between 48° and 50°
  3. customare obtained

Sources & evidence

ORD record
ord-f0d522195d664d27aa892290571010f9
Source dataset
uspto-grants-1979_06
Patent number
US04157399

Reaction notes

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